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1 article(s) from Mayhugh, Amy L

Room-temperature Pd/Ag direct arylation enabled by a radical pathway

Amy L. Mayhugh and
Christine K. Luscombe

Beilstein J. Org. Chem. 2020, 16, 384–390, doi:10.3762/bjoc.16.36

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Scheme 1: A high yielding, highly selective room-temperature direct arylation reaction between indole and iod...

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Figure 1: ¹H NMR (500 MHz, CDCl₃) of (a) 5-iodo-1-octylindole monomer (b) PIn prepared according to condition...

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Figure 2: MALDI–TOF MS of PIn, indicating octylindole repeat units with three different types of end groups. ...

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Scheme 2: Commonly discussed mechanisms for C2 selective direct arylation, none containing radical intermedia...

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Scheme 3: Proposed mechanism for palladium radical involved reaction between indole and iodobenzene.

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Scheme 4: Radical trap effects on literature methods for the direct arylation at room temperature. A) From re...

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Published 13 Mar 2020

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